How to Check Dapoxetine Powder Quality: COA, HPLC, and MSDS Explained

内容目录


Introduction

When sourcing Dapoxetine Hydrochloride (HCl) powder, price alone should never determine supplier choice. The global API market is flooded with suppliers, and while some provide GMP-certified, high-purity product, others ship adulterated, low-grade, or mislabeled powders.

To avoid costly mistakes, buyers must know how to verify quality before scaling orders. The three cornerstones of verification are:

  1. COA (Certificate of Analysis) – confirms batch specifications.
  2. HPLC (High Performance Liquid Chromatography) – verifies purity and identity.
  3. MSDS (Material Safety Data Sheet) – ensures safety, handling, and compliance.

This guide explains how to use these documents and tests to confirm the authenticity of Dapoxetine powder.

👉 For procurement strategy, see the Complete 2025 Buyer’s Guide to Dapoxetine HCl Powder.


Step 1: Reviewing the COA

A Certificate of Analysis (COA) is the first checkpoint in verifying a Dapoxetine shipment. Every supplier should provide a COA for the exact batch delivered.

Key COA Fields to Check

  • Product Name & CAS No.: Dapoxetine HCl, CAS 129938-20-1
  • Batch Number & Date: Ensures traceability
  • Appearance: White to off-white crystalline powder
  • Assay (Purity): ≥99% (HPLC method)
  • Loss on Drying (LOD): ≤0.5%
  • Heavy Metals: <10 ppm
  • Residual Solvents: Within ICH Q3C limits

📌 Tip: COAs can be falsified. Always request third-party lab test results or run your own verification.

👉 Supplier comparisons available in Top Dapoxetine Powder Manufacturers & Suppliers 2025.


Step 2: Confirming with HPLC Testing

Even with a COA in hand, independent HPLC (High Performance Liquid Chromatography) analysis is critical.

Why HPLC Matters

  • Confirms chemical identity (retention time compared to standard Dapoxetine).
  • Detects impurities and degradation products.
  • Quantifies purity percentage (≥99% expected).

Best Practices

  • Send 100 g sample lot to an accredited third-party lab.
  • Verify chromatogram peaks match Dapoxetine reference standard.
  • Reject batches with unidentified peaks or purity <99%.

📊 Industry norm: Top GMP factories report Dapoxetine HCl purity between 99.0–99.5% HPLC.

👉 For long-term procurement, see Wholesale & Bulk Dapoxetine Powder Supply.


Step 3: Using the MSDS for Compliance

A Material Safety Data Sheet (MSDS) ensures safe handling, storage, and transport. Customs and regulatory agencies also require MSDS documentation for import/export.

Critical MSDS Sections

  • Identification: Product name, CAS number, synonyms
  • Hazard Classification: Irritant; toxic if misused
  • First Aid Measures: Guidance for inhalation, ingestion, skin/eye exposure
  • Handling & Storage: Store at 2–8°C, dry, sealed, away from light
  • Transport Information: HS Code 29339990; shipping class not hazardous, but regulated as API

⚠️ Missing or incomplete MSDS is a red flag — shipments may be delayed or rejected at customs.

👉 For full template, see Dapoxetine Powder MSDS & Safety Guidelines.


Additional Verification Methods

  1. NMR (Nuclear Magnetic Resonance): Confirms molecular structure.
  2. IR Spectroscopy: Matches fingerprint region with Dapoxetine reference.
  3. Particle Size Distribution: Important for micronized batches.
  4. Stability Testing: Ensures 24–36 month shelf life under 2–8°C storage.

Buyer Red Flags

  • Supplier refuses to provide COA or MSDS.
  • COA reports exactly 100.0% purity (unrealistic, often fake).
  • No batch number or manufacturing date on documents.
  • Refusal to send samples for third-party testing.
  • Quotes below $250/kg bulk (high probability of counterfeit).

Conclusion

Verifying Dapoxetine HCl powder quality is essential for avoiding financial loss, regulatory issues, and product failure.

Key steps:

  • Start with COA review → look for ≥99% HPLC purity.
  • Confirm via third-party HPLC test.
  • Ensure a valid MSDS accompanies every batch.
  • Use NMR, IR, and stability tests for advanced verification.

📌 Next Steps:

By combining document review, analytical testing, and supplier audits, buyers can ensure every shipment of Dapoxetine powder meets pharma-grade standards.

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